Key equations for Process EngineersPhase separation乐动安卓Solved Sample Problems

样品问题 - 液体液体分离器尺寸带有Demsiter Pad

Problem Statement

Perform separator sizing calculations for a vertical gas-liquid separator used for separation of fuel gas bubbles entrained in water flow.
水流= 18 m3/hr
Entrained Flow of fuel gas = 100 m3/hr
Operatingtemperatureof separator = 250C
Operatingpressureof separator = 0.2 barg (near atmospheric)
Separation efficiency required is to remove 80% of gas bubbles above the size of 10 microns.
汽油gas properties can be approximately taken as properties of ethane

Size the drum as (i) an empty vessel and (ii) vessel with demister pad with K=0.1 m/s for removing 100 micron droplet size. Compare the minimum vessel size requirements in both the cases.

Solution

For the case (i), separator sizing of two phase separator as an empty vessel is performed inEnggCyclopedia's solved sample problem. This type of separator relies only on gravity settling of liquid droplets and requires sufficient residence time for the gas phase so that the liquid droplets can settle down. This often results in a large vessel for separation of small liquid droplets.

A除雾器垫assists the separation of liquid droplets by impinging liquid droplets into each other to from bigger drops which are too heavy to rise with the gas and drop down into the pool of liquid in the separator.

For gas liquid separators, following equation for the gas phase design velocity governs the separator diameter,

ρLand ρG是the densities of liquid and gas phase respectively.

K is a proportionality constant which depends on a number of factors which include liquidviscosity, surface tension, entrainment loading, and the content of dissolved and suspended solids. For our sample problem, we know the 'K' value to be 0.1 m/s for removing 100 micron size liquid droplets.

It shoud be noted that the 'K' value is directly proportional to the square of the droplet size to be knocked out from gas. Hence for 10 micron size particles, 'K' calue is estimated as,

k = 0.1×(10/100)2= 10-3Thus the separator sizing can be performed in following basic steps.

Step1

density在25岁0C = 994.72 kg/m3
viscosity在25岁0C = 0.9 CP
For fuel gas properties,
Molecular weight of ethane = 30 gm/gmole
汽油气体密度在25岁0C = 1.45 kg/m3
汽油gas viscosity at 250C = 0.0069 cP

步骤2

The design velocity for gas phase is calculated as follows,

with K = 10-3,ρL= 994.72 kg/m3and ρG= 1.45 kg/m3

Vt= 10-3×√((994.72-1.45)/1.45)= 2.6×10-2m/s

This design velocity for gas phase is related to the drum diameter as,

Vt= 4×Vg/(3600×πd2)... where Vg is gas volumetric flow (m3/hr) and 'd' is vessel diameter

因此,

d = √Vg/(900×π×Vt)

d = √100/(900×π×2.6×10-2) = 1.166 m

Compared to minimum drum diameter requirement of 2.13 m for empty vertical KO Drum which only relies on gravity settling for separation of liquid droplets. It can be readily observed that drum size is reduced by 15% in terms of drum diameter by using a demister pad.

Using the L/D ratio of 3.5 ,

L = 3.5 × 1.17 = 4.095 m

必须检查此长度以符合液体的项目规范residence time between HLL and LLL.If the length is not sufficient to provide enough residence time between HLL and LLL, then the length can be increased along with the diameter by resepcting the L/D ratio constraints.

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